Polyfunctional biocompatible hydrogel and method for the...

A - Human Necessities – 61 – L

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A61L 27/16 (2006.01) A61L 27/52 (2006.01)

Patent

CA 2461821

The inventive polyfunctional biocompatible hydrogel comprises 1.3-1.5 mass % of acrylamide, 0.004-0.975 mass % of cross-linking agents-N,N'-methylene-bis- acrylamide, 0.004-5.1 mass % of N,N'-ethylene-bis-acrylamide, 0.002-0.45 mass % of poviargol and water up to 100 mass %. Said hydrogel is produced by co- polymerising acrylamide with the cross-linking agents in an aqueous medium in the presence of peroxide polymerisation initiator, the incubation of reaction mixture being carried out in two stages. The first stage is carried out at a temperature ranging from 20 to 90° C. during a time of 2 to 24 hours, the second stage being carried out at a temperature ranging from 107 to 130° C. during a time equal to or less than 2 hours.

L'invention concerne un hydrogel biocompatible polyfonctionnel contenant de 1,3 à 15 % en masse d'acrylamide, de 0,004 à 0,975 % en masse d'agents de réticulation N,N'-méthylène-bis acrylamide, de 0,004 à 5,1 % en masse de N,N'-éthylène-bis-acrylamide, de 0,002 à 0,45 % en masse de poviargol, et le reste en eau. L'hydrogel selon l'invention est obtenu par copolymérisation d'acrylamide au moyen desdits agents de réticulation, dans un milieu aqueux, en présence d'un initiateur peroxyde de polymérisation, l'incubation du mélange de réaction s'effectuant en deux étapes. La première étape est réalisée à une température comprise entre 20 et 90 ·C, pendant une durée comprise entre 2 et 24 heures, et la deuxième étape est réalisée à une température comprise entre 107 et 130 ·C, pendant une durée inférieure à 2 heures.

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