Polyoxometalate intercalated layered double hydroxides

Details Polyoxometalate intercalated layered double hydroxides Polyoxometalate intercalated layered double hydroxides

C - Chemistry, Metallurgy

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C01G 1/02 (2006.01) B01J 20/02 (2006.01) B01J 21/16 (2006.01) B01J 23/00 (2006.01) B01J 29/04 (2006.01) C01B 13/14 (2006.01) C01F 7/00 (2006.01)

Patent

CA 2063731

This disclosure describes the synthesis of layered double hydroxide compositions interlayered by polyoxometalate anions with Keggin-type structures and having the formula [M1-x"Mx'''(OH)2]Ax/n-.yH2O, wherein, M'' is a divalent metal and M''' is a trivalent metal, A is an anionic polyoxometalate of negative charge n, x range between 0.12 to 0.8, and y is a positive number. The products exhibit well-defined XRD peaks corresponding to uniformly crystalline layered products with basal spacing values > 14 .ANG..

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