Preparation of 2-(3-methylpiperidinothio)-benzothiazole and...

Details Preparation of 2-(3-methylpiperidinothio)-benzothiazole and... Preparation of 2-(3-methylpiperidinothio)-benzothiazole and...

C - Chemistry, Metallurgy

07

D

260/277.7

C07D 401/12 (2006.01) C07D 211/54 (2006.01) C07D 277/80 (2006.01) C08K 5/47 (2006.01)

Patent

CA 1065320

INVENTORS: Richard Leshin, Penelope R. Pappas and Dane K. Parker INVENTION: PREPARATION OF 2-(3-METHYLPIPERIDINOTHIO)- BENZOTHIAZOLE AND 2-(4-METHYLPIPERIDINOTHIO)- BENZOTHIAZOLE Abstract of the Disclosure This invention relates to an improved procsss for preparing 2-(3-methylpiperidinothio)-benzothiazole and 2- (4-methylpiperidinothio)-benzothiazole wherein the order of addition of the reactants comprises slurrying benzothiazolyl disulfide in water, adding an oxidizing agent and effecting a reaction by the addition of an amine or an amine salt solution.

233629

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