Preparation of 3-mercaptopropionitrile and...

C - Chemistry – Metallurgy – 07 – C

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C07C 319/06 (2006.01) C07C 319/12 (2006.01) C07C 323/25 (2006.01) C07C 323/52 (2006.01) C07C 323/60 (2006.01)

Patent

CA 2146626

Facile process for the production of 3-mercaptopropionitrile and 3-mercaptopropionic acid by reacting thiodipropionitrile with alkaline hydrosulfide in the presence of alkaline hydroxide. Acidification of the resulting reaction product with a strong acid, or saponification, yields the desired mercaptopropionic acid, which can be isolated in high yield.

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