Preparation of an allyl amine and quaternary diallyl...

Details Preparation of an allyl amine and quaternary diallyl... Preparation of an allyl amine and quaternary diallyl...

C - Chemistry, Metallurgy

07

C

260/594, 260/606

C07C 209/12 (2006.01) C07C 209/08 (2006.01) C07C 211/21 (2006.01) C07D 295/023 (2006.01)

Patent

CA 1288105

ABSTRACT An allyl amine compound such as an allyl dialkyl amine is prepared by the reaction of ammonia or a water soluble amine with an allyl halide in the presence of an alkali metal or alkaline earth metal hydroxide or carbonate using a two-phase reaction system comprising water and a water- -immiscible organic liquid. The allyl amine pro- duct is of an exceptionally high purity and con- tains relatively small amounts of salt. When the reaction method is employed to prepare an allyl dialkyl amine, the allyl dialkyl amine can effec- tively be quaternized to prepare a pure diallyl dialkyl ammonium compound at high yields.

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