Preparation of an anhydrous quinoline-based cetp inhibitor...

Details Preparation of an anhydrous quinoline-based cetp inhibitor... Preparation of an anhydrous quinoline-based cetp inhibitor...

C - Chemistry, Metallurgy

07

D

C07D 215/00 (2006.01) C07D 215/42 (2006.01)

Patent

CA 2461686

This invention relates to methods for preparing anhydrous CETP inhibitor, (2R, 4S)-4-[(3,5-bis-trifluoromethyl-benzyl)-methoxycarbonyl-amino]-2-ethyl-6- trifluoromethyl-3,4-dihydro-2H-quinoline-1-carboxylic acid ethyl ester by crystallization.

L'invention concerne des procédés de préparation d'un inhibiteur CETP anhydre, soit de l'ester éthylique d'acide (2R, 4S)-4-[(3,5-bis-trifluorométhyl-benzyl)-méthoxycarbonyl-amino]-2-éthyl-6-trifluorométhyl-3,4-dihydro-2H-quinoline-1-carboxylique, par cristallisation.

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