Preparation of bis-2-pyridyl-disulfides

C - Chemistry – Metallurgy – 07 – D

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260/277.8

C07D 401/12 (2006.01) C07D 213/71 (2006.01) C07D 213/89 (2006.01)

Patent

CA 1117116

ABSTRACT OF THE DISCLOSURE In a process for the preparation of bis-2- pyridyl-disulfide or bis-(2-pyridyl-1-oxide)-disulfide optionally substituted on the pyridyl ring with at least one substituent selected from the group consisting of halogen and alkyl and alkoxy of 1 to 4 carbon atoms by oxidation of the corresponding 2-mercapto-pyridine or its N-oxide, the improvement comprising effecting the oxidation in an aqueous acid media containing an alkali metal or alkaline earth metal chlorite.

341923

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