Preparation of deuterated methylene chloride

Details Preparation of deuterated methylene chloride Preparation of deuterated methylene chloride

C - Chemistry, Metallurgy

07

B

260/659

C07B 59/00 (2006.01) C07C 19/02 (1990.01)

Patent

CA 1283131

64725-433 ABSTRACT OF THE DISCLOSURE A process for the preparation of deuterated methylene chloride. The process comprises contacting methylene chloride with an aqueous phase containing deuteroxide ions in the presence of a phase-transfer catalyst. Deuterated methylene chloride is of importance as an industrial and research reagent and as a solvent in NMR spectroscopy.

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