Preparation of dien-1-o1s, 9-hydroxydodec-10-enyl...

Details Preparation of dien-1-o1s, 9-hydroxydodec-10-enyl... Preparation of dien-1-o1s, 9-hydroxydodec-10-enyl...

C - Chemistry, Metallurgy

07

C

260/631.5

C07C 33/02 (2006.01) C07C 29/10 (2006.01) C07C 29/60 (2006.01) C07C 43/178 (2006.01)

Patent

CA 1311502

- 20 - O.Z. 0050/39405 Abstract of the Disclosure: Dien-1-ols of the general formula I (I) Image where the radicals R1 to R7 are identical to or different from one another and each is hydrogen or straight-chain or branched alkyl of 1-12 carbon atoms and n is 1-14, are prepared by dehydrating a hydroxyalkenyl tert-butyl ether of the formula II (II) Image in the presence of an acidic catalyst at elevated tem- peratures and essentially at the same time splitting off the tert-butyl protective group, as is 9-hydroxydodec-10- enyl 1-tert-butyl ether which is useful as an intermedi- ate for synthesizing 8,10-dodecadienol.

575015

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