Preparation of double metal cyanide-catalyzed polyols by...

C - Chemistry – Metallurgy – 08 – G

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C08G 65/10 (2006.01) C08G 18/08 (2006.01) C08G 18/48 (2006.01) C08G 65/26 (2006.01)

Patent

CA 2245563

Double metal cyanide-catalysed polyols are made by an improved process in which a starter is continuously added during polymerization of the epoxide. The process includes a continuously added starter (S c), and optionally, an initially charged starter (S i). The continuously added starter comprises at least about 2 equivalent percent of the total starter used. The process enables the use of water and low molecular weight polyol starters in DMC-catalyzed polyol synthesis. In addition, the process gives polyether polyols having reduced levels of high molecular weight polyol tail, which can adversely affect polyurethane foam processing.

On prépare des polyols catalysés au moyen d'un catalyseur double métal au cyanure (DMC) selon un procédé amélioré consistant à effectuer l'apport en continu d'un initiateur pendant la polymérisa tion de l'époxyde. Ce procédé implique l'addition en continu d'un initiateur (Sc) et, éventuellement, l'utilisation d'un initiateur chargé initialement (Si). Ce dernier représente au moins environ 2 % en équivalence de la totalité de l'initiateur utilisé. Ce procédé permet d'utiliser de l'eau et des initiateurs de poly ols à poids moléculaire bas dans la synthèse de polyols catalysés par DMC. De plus, ce procédé permet d'obtenir des polyols de polyéther possédant des teneurs limitées en queue de polyol à poids moléculaire élevé, laquelle pourrait autrement avoir un effet négatif sur le traitement de la mousse de polyuréthane.

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