Preparation of ion-exchange catalysts

Details Preparation of ion-exchange catalysts Preparation of ion-exchange catalysts

B - Operations, Transporting

01

J

402/2

B01J 31/08 (2006.01) B01J 47/00 (2006.01) C07D 277/04 (2006.01)

Patent

CA 1258342

ABSTRACT This invention is a process for preparing an insoluble strong-acid cation-exchange resin in acid form modified by the partial neutralization of its cation- -exchange capacity with aminoalkanethiol. The process is characterized by contacting the cation-exchange resin with an N-(2-mercaptoalkyl)amide in the presence of water under reaction condition sufficient to produce the modi- fied cation-exchange resin. The partially neutralized resin can be treated further by contacting it with an aldehyde or ketone under reaction conditions sufficient to convert the aminoalkanethiol moieties to thiazolidine moieties. These partly neutralized resins are useful as catalysts in the preparation of bisphenols from phenol and carbonyl compounds.

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