Preparation of monoepoxides

Details Preparation of monoepoxides Preparation of monoepoxides

C - Chemistry, Metallurgy

07

D

260/371

C07D 301/02 (2006.01) C07D 301/26 (2006.01) C07D 303/08 (2006.01)

Patent

CA 2026866

ABSTRACT Monoepoxides are prepared by a process which comprises (1) continuously or intermittently contacting a mixture of (a) a compound having only one vicinal halohydrin moiety per molecule and (b) at least one solvent having a boiling point at least about 10°C above the boiling point of the monoepoxide being produced and which is essentially non-reactive with any of the compounds in the reaction mixture with (c) an aqueous solution of an alkali metal hydroxide; (2) continuously removing by codistilling or azeotroping a mixture of water and resultant vicinal epoxide-containing compound from the reaction mixture; and (3) separating the vicinal epoxide-containing compound from the water by any suitable means. 37,726-F

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