Preparation of particulate radioactive waste mixtures

G - Physics – 21 – F

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G21F 9/16 (2006.01) B01F 7/08 (2006.01) B01F 13/10 (2006.01) C04B 35/645 (2006.01)

Patent

CA 1288586

ABSTRACT OF THE DISCLOSURE A dry, pourable particulate mixture of nuclear waste and synthetic rock-forming components is produced by supplying the rock forming components in dry particulate form to a mixer, supplying the nuclear waste in liquid phase and operating the mixer to distribute the waste substantially uniformly through the synthetic rock components; the mixture is calcined to produce a precursor powder which is adapted to be used in a hot pressing process to form synthetic rock throughout which the radioactive nuclear waste is distributed and immobilised. A reducing gas atmosphere is preferably maintained in the calcining process stage, the gas being for example pure hydrogen or a mixture of hydrogen in nitrogen in proportions which are non-explosive. A screw type or paddle type conveyor can be used for the mixing and calcining stages although the calcining can be effected in a vertically downwardly directed tube device having associated heating means such as microwave heating.

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