Preparation of solid, free-flowing water-soluble salts of...

C - Chemistry – Metallurgy – 07 – C

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C07C 59/70 (2006.01) A01N 39/02 (2006.01) A01N 39/04 (2006.01) C07C 51/41 (2006.01)

Patent

CA 2208538

A process is disclosed for preparing solid, free-flowing water-soluble salts of aryloxy-C1-C4-alkane carboxylic acids. Aryloxy-C1-C4-alkane carboxylic acids are reacted with a salt-forming base. Salts are formed in the melt in the presence or absence of an entrainer suitable for causing azeotropic water separation or in a solution in the presence of an entrainer suitable for causing azeotropic water separation. The entrainer is removed from the reaction mixture during or after the reaction and the solid salts are then isolated in the usual manner.

Selon un procédé de préparation de sels solides à écoulement libre solubles dans l'eau d'acides aryloxy-alcane-C1-C4-carboxyliques, on fait réagir les acides aryloxy-alcane-C1-C4-carboxyliques avec une base formatrice de sels. Les sels se forment dans la masse fondue en présence ou en l'absence d'un agent entraîneur apte à provoquer la séparation azéotrope de l'eau ou dans une solution en présence d'un agent entraîneur propre à entraîner la séparation azéotrope de l'eau. L'agent entraîneur est enlevé du mélange de réaction pendant ou après la réaction, puis les sels solides sont isolés de la manière usuelle.

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