Process and apparatus for making p.sub.2s.sub.5 of low...

C - Chemistry – Metallurgy – 01 – B

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23/79

C01B 25/14 (2006.01)

Patent

CA 1139077

PROCESS AND APPARATUS FOR MAKING P2S5 OF LOW REACTIVITY ABSTRACT OF THE DISCLOSURE: The invention relates to a process for making phospho- rus pentasulfide of low reactivity. To this end, molten phosphorus pentasulfide is solidified and the solidified product is ground. More specifically, solid phosphorus pentasulfide coming from a cooling zone with a tempe- rature of 150 to 220°C is introduced into a heat-insula- ted tank and freed therein from its immanent heat by controlled cooling at a rate of at most 30°C/h. The inven- tion also relates to an apparatus for carrying out this process.

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