Process and apparatus for producing substituted thiocarbamates

B - Operations – Transporting – 01 – J

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23/385, 260/467.

B01J 8/34 (2006.01) C07C 155/02 (1980.01)

Patent

CA 1113106

ABSTRACT OF THE DISCLOSURE: Substituted thiocarbamates are produced by contin- uously feeding together a secondary amine and sulphur in stoi- chiometric propertions and in a suitable solvent into a reaction colum subjected to pressure by carbon monoxide. A continuous circulation of the reaction solution is maintained in the co- lumn, and the effluent is subjected to alkylation, the substi- tuted carbamate being derived therefrom continuously.

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