Process and composition for the preparation of transparent...

C - Chemistry – Metallurgy – 08 – G

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C08G 18/10 (2006.01) C08G 18/12 (2006.01) C08G 18/44 (2006.01) C08G 18/75 (2006.01)

Patent

CA 2617686

A process for the preparation of transparent polyurethanes is disclosed, comprising step a) of preparing a prepolymer by reaction of one or more aliphatic or cycloaliphatic isocyanates, having two or more isocyanate groups, and one or more polyhydroxy compounds, having two or more hydroxy groups and a molecular weight ranging from 150 to 2000, step b) of preparing a composition comprising one or more polyhydroxy compounds, having two or more hydroxy groups and a molecular weight ranging from 150 to 2000 and a functionality from 2 to 5, and a suitable catalyst, and step c) of reacting the so-obtained prepolymer with the composition of step b), wherein at the end of step a) the percentage of free isocyanate groups in the prepolymer is at least 15%. In the preferred disclosed process, the percentage of free isocyanate groups in the prepolymer is from 15 to 30%. Particularly, a composition for the preparation of transparent polyurethanes and polyurethanes obtainable by said process are disclosed.

L~invention concerne un procédé de préparation de polyuréthanes transparents, comprenant l~étape a) de préparation d~un prépolymère par réaction d~un ou plusieurs isocyanates aliphatiques ou cycloaliphatiques ayant deux groupes isocyanates ou plus et un composé polyhydroxy ou plus ayant deux groupes hydroxy ou plus et un poids moléculaire dans la gamme de 150 à 2000, l~étape b) de préparation d~une composition comprenant un composé polyhydroxy ou plus ayant deux groupes hydroxy ou plus et un poids moléculaire dans la gamme de 150 à 2000 et une fonctionnalité de 2 à 5, et un catalyseur approprié, et l~étape c) de réaction du prépolymère ainsi obtenu avec la composition de l~étape b), où à la fin de l~étape a) le pourcentage de groupes isocyanates libres dans le prépolymère est au moins de 15 %. Dans le procédé préféré selon l~invention, le pourcentage de groupes isocyanates libres dans le prépolymère est de 15 % à 30 %. L~invention concerne en particulier une composition pour la préparation de polyuréthanes transparents et les polyuréthanes qu~il est possible d~obtenir à partir dudit procédé.

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