Process and device for purifying chemical substances

B - Operations – Transporting – 01 – J

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B01J 2/06 (2006.01) B01D 9/00 (2006.01) B01J 2/00 (2006.01) B01J 2/22 (2006.01) B01J 2/26 (2006.01)

Patent

CA 2165476

Wash columns as used to remove impurities from the residual melt from melt crystallization are of limited efficiency due to the fact that the crystal mass normally fed in contains solids of different sizes, which partially also tend to agglomerate. The purifying action based on the flow around these solid components is therefore limited. The invention proposes to load wash columns with monodisperse particles produced beforehand by means of suitable granulators. The invention also relates to the use of this process and of this device for purifying and preparing chemical substances.

Les colonnes de lavage, telles qu'on les utilise pour enlever des impuretés de la masse en fusion résiduelle, lors de la cristallisation par fusion, sont d'une efficacité limitée étant donné que la masse cristalline normalement introduite comprend des solides de différentes tailles qui, en partie, ont tendance à s'agglomérer. L'effet de purification qui repose sur l'écoulement d'un flux autour de ces solides est donc limité. Il est proposé, selon l'invention, de charger les colonnes de lavage avec des particules monodispersées produites à l'avance au moyen de granulateurs appropriés. L'invention concerne également l'utilisation de ce procédé et d'un tel dispositif pour purifier et préparer des substances chimiques.

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