Process for demetallizing primary products of the oxo synthesis

C - Chemistry – Metallurgy – 07 – C

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260/574, 23/395.

C07C 47/02 (2006.01) B01J 19/14 (2006.01) B01J 31/40 (2006.01) C07C 29/16 (2006.01) C07C 45/50 (2006.01)

Patent

CA 1150314

ABSTRACT OF THE DISCLOSURE An improved process for de-cobaltizing the primary product of an oxo synthesis is disclosed wherein the primary product is contacted with steam introduced into a vessel to which the primary oxo product is introduced but initially maintained in out of contact relationship to such product by a cooling medium whereby heat transfer from the steam to the primary product is initially avoided. The primary product and steam are fed to a cylindrical reactor having a conical base, and after the steam has risen 1/2 to 2/3 of the height of the conical base it comes in contact with the primary product whose liquid level height in the vessel is maintained at one to two times the vessel's diameter An apparatus for performing such process is also disclosed.

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