Process for distillation of crude isocyanate concentrates

Details Process for distillation of crude isocyanate concentrates Process for distillation of crude isocyanate concentrates

C - Chemistry, Metallurgy

07

C

260/496.1

C07C 263/20 (2006.01)

Patent

CA 2028819

2028819 9009990 PCTABS00002 A process is described for the separation and recovery of isocyanate monomers from isocyanate concentrates which leaves a residue which is liquid and burnable. The process for the separation and recovery of isocyanate monomers from isocyanate concentrates formed in the production of isocyanates and comprising a volatile isocyanate monomer and by-products comprises the steps of: (A) preparing a mixture comprising (A-1) the isocyanate concentrate; and (A-2) an oil solution comprising; (A-2-a) a major amount of hydrocarbon oil, and (A-2-b) a minor amount of at least one ashless dispersant; and (B) heating the mixture to an elevated temperature at reduced pressure whereby isocyanate monomer is distilled and recovered leaving a liquid residue. The presence of the oil solution in the mixture facilitates the distillation of the isocyanate concentrate, generally improves the yield of distilled isocyanate monomer, results in a residue which is liquid and easily removed from the distillation apparatus, and the liquid residue can generally be burned without difficulty.

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