Process for lignin recovery

C - Chemistry – Metallurgy – 07 – D

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C07D 307/50 (2006.01) D21C 11/00 (2006.01) C07G 1/00 (2006.01) C08H 6/00 (2010.01)

Patent

CA 1267648

- 18 - ABSTRACT OF THE DISCLOSURE Lignin is precipitated in high yields and at high rates from a black liquor produced by pulping wood at high temperatures and pressures with an aqueous lower aliphatic alcohol solvent. The lignin is precipitated by diluting the black liquor with water and an acid to form a solution with a pH of less than about 3, an alcohol content of less than about 30% by volume and a tempera- ture of less than about 60°C. The precipitated lignin, when subsequently dried, is in the form of a powder which requires little or no crushing to convert it into a fine uniform size suitable for use without further significant processing.

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