Process for making aluminosilicate for record material

C - Chemistry – Metallurgy – 01 – B

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C01B 33/26 (2006.01) B41M 5/155 (2006.01) C09C 1/40 (2006.01)

Patent

CA 2164208

A process for the production of an aluminosilicate containing at least 9 weight percent alumina, having a BET surface area of 300-600 m2/g, and an average pore volume of 0.2-0.5 ml/g is disclosed. The process includes the steps of preparing an aqueous solution comprising at least one metal silicate, adjusting the pH of said aqueous solution comprising at least one metal silicate with a sufficient amount of an aqueous solution comprising at least one aluminum salt to produce an aqueous solution having a pH of 4.4-7.7, precipitating aluminosilicate from the aqueous solution by concurrently dosing additional aqueous solution comprising at least one metal silicate in such a manner such that the pH is maintained at 4.4-7.7, steps (a)-(c) being carried out at a temperature of 0-80 °C and isolating said aluminosilicate. The aluminosilicate is useful as a pressure sensitive pigment in carbonless copy paper.

Procédé de production d'un aluminosilicate contenant au moins 9 % en poids d'alumine, présentant une surface BET comprise entre 300 et 600 m<2>/g, et un volume poreux moyen compris entre 0,2 et 0,5 ml/g. Ce procédé consiste à préparer une solution aqueuse comprenant au moins un silicate métallique, à ajuster le pH de la solution aqueuse comprenant au moins un silicate métallique à l'aide d'une quantité suffisante d'une solution aqueuse comprenant au moins un sel d'aluminium pour produire une solution aqueuse d'un pH compris entre 4,4 et 7,7, à précipiter l'aluminosilicate de la solution aqueuse par dosage simultané d'une solution aqueuse supplémentaire comprenant au moins un silicate métallique, de manière à maintenir le pH à un niveau compris entre 4,4 et 7,7, les étapes (a) à (c) étant exécutées à une température comprise entre 0 et 80 DEG C, et à isoler l'aluminosilicate. Ledit aluminosilicate se prête à une utilisation comme pigment sensible à la pression dans du papier autocopiant sans carbone.

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