Process for making calcium sulfate alpha-hemihydrate from...

C - Chemistry – Metallurgy – 01 – F

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C01F 11/46 (2006.01) A01K 1/015 (2006.01) C04B 11/02 (2006.01) C04B 11/024 (2006.01) C04B 11/26 (2006.01) C04B 18/02 (2006.01) C04B 22/14 (2006.01) E04F 15/12 (2006.01)

Patent

CA 1335034

The process makes calcium sulfate alpha-hemihydrate from finely divided calcium sulfate dihydrate by transforming the calcium sulfate dihydrate in the presence of saturated steam. A molded body is formed from the calcium sulfate dihydrate which has a plurality of pores having a pore volume amounting to 15 to 60 % by volume of the total volume of the entire molded body. More than 5 % by volume of the pore volume contains air. The molded body is fed to the autoclave. In the presence of a sufficient water quantity in the pores the crystal habit and the crystal growth of the calcium sulfate alpha-hemihydrate crystals which grow in an aqueous solution phase are controlled by a process temperature in the range between 110° to 180°C by the pressure of the process atmosphere in the autoclave. The molded body is removed from the autoclave after recrystallization transformation and delivered for use. Key products of this process and their derivatives are also described.

567517

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