Process for making methylcyclopentadienyl manganese...

Details Process for making methylcyclopentadienyl manganese... Process for making methylcyclopentadienyl manganese...

C - Chemistry, Metallurgy

07

F

260/428.1

C07F 13/00 (2006.01)

Patent

CA 2034046

Cyclopentadienyl manganese tricarbonyl compounds are made by reacting a mixture of 0.25-0.55 mole of manganese acetate and 0.45-0.55 mole of a bis-cyclopentadienyl manganese compound with 0.5-2.1 moles of an alkyl aluminum compound (e.g., triethyl aluminum) in the presence of 0.75-1.25 moles of an ether per mole of said alkyl aluminum compound and reacting the mixture with carbon monoxide at 65-175°C and 300-2500 psig.

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