C - Chemistry – Metallurgy – 01 – B
Patent
C - Chemistry, Metallurgy
01
B
23/195
C01B 21/068 (2006.01) C30B 25/00 (2006.01)
Patent
CA 2000457
Silica powder or a mixture of silica powder and silicon nitride whisker are heated at a temperature ranging from 800°C to 1,700°C in a gaseous mixture of ammonia gas (NH3) and hydrocarbon gas (CmHn) so as to produce silicon nitride whisker. The gaseous mixture flows at the rate of 10 mm/sec or less. The ratio of the ammonia to the hydrocarbon expressed as NH3/CH4 ranges from 0.5:1 to 2000:1 by volume. The silica powder is preferably mixed with at least one of six catalysts: transition metals; alkali metals: alkaline earth metals: halides of transition metals; halide; of alkali metals; and alkaline earth metals. One mol part of the silica powder is mixed with 0.001 - 1.0 mol part of the catalyst.
Imai Isao
Ishii Toshitsugu
Sueyoshi Kouichi
Smart & Biggar
Toshiba Ceramics Co. Ltd.
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