Process for manufacturing alkylphosphonate monoesters

Details Process for manufacturing alkylphosphonate monoesters Process for manufacturing alkylphosphonate monoesters

C - Chemistry, Metallurgy

07

F

C07F 9/40 (2006.01) C10M 137/12 (2006.01)

Patent

CA 2456752

The present invention discloses a process for manufacturing an alkylphosphonate monoester. The process may comprise partially hydrolyzing an alkyl phosphate diester with an alkaline compound in a first solvent to provide a reaction mixture, wherein the first solvent comprises a mixture of an alcohol and water. The reaction mixture may be diluted with a second solvent to provide an organic phase, wherein the second solvent comprises at least one non-polar organic solvent. The process may comprise acidifying the reaction mixture with an acid, wherein the organic phase includes an alkylphosphonate monoester.

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