Process for preparation of carbon fibers having structure...

D - Textiles – Paper – 01 – F

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18/506, 18/6

D01F 9/12 (2006.01) D01F 9/00 (2006.01) D01F 9/145 (2006.01)

Patent

CA 1173608

PROCESS FOR PREPARATION OF CARBON FIBERS HAVING STRUCTURE REFLECTED IN CROSS SECTIONAL VIEW THEREIN AS RANDOM MOSAIC ABSTRACT OF THE DISCLOSURE; A process is described for preparation of carbon fibers wherein pitch fibers are prepared from a mesophase-pitch containing not more than 80% by weight of a quinoline- insoluble component and showing, under a polarization microscope, more than 70 % of optically anisotropic region, comprising the steps of subjecting a mesophase-pitch having a viscosity of 10 to 100 poise at a spinning temperature of 330 to 450°C, to rotating-centrifugal-spinning in a rotating-centrifugal spinning machine with a nozzle periph- eral velocity of 300 to 1000 m/min and exposing the thus spun mesophase pitch fibers to a flow of a gas in the spinning direction at a temperature of 280 to 400°C and at a linear velocity of 50 to 200 m/sec, thereby prepar- ing pitch fibers showing a random mosaic cross sectional pattern. The pitch fibers are then converted to carbon fibers by infusibilization, carbonization and graphitization.

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