Process for preparing 2-(1-cyclohexenyl)-cyclohexanone

Details Process for preparing 2-(1-cyclohexenyl)-cyclohexanone Process for preparing 2-(1-cyclohexenyl)-cyclohexanone

C - Chemistry, Metallurgy

07

C

260/582.5

C07C 49/385 (2006.01) C07C 45/74 (2006.01) C07C 49/613 (2006.01)

Patent

CA 1067100

ABSTRACT OF THE DISCLOSURE 2-(1-cyclohexenyl)-cyclohexanone is prepared by condensation of cyclohexanone using a macro-porous ion exchange resin such as Lewatite SPC 118 W or equivalent at temperatures not exceeding 125 °C., provided that the conversion reaction is maintained below 50 %, preferably below 35 %. The reaction mixture is distilled at atmospheric pressure in the absence of the ion exchange resin and the desired product is recovered in substantially high yields generally greater than 95 %. - 1 -

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