Process for preparing catalysts for producing methacrylic acid

Details Process for preparing catalysts for producing methacrylic acid Process for preparing catalysts for producing methacrylic acid

B - Operations, Transporting

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252/51.D

B01J 27/19 (2006.01) B01J 23/885 (2006.01) B01J 27/199 (2006.01) B01J 37/00 (2006.01) B01J 37/12 (2006.01) C07C 51/25 (2006.01) C07C 57/04 (2006.01)

Patent

CA 2027323

In a process for producing a catalyst having a composition represented by the following formula usable to produce methacrylic acid by the gas-phase catalytic oxidation of methacrolein with molecular oxygen, P a Mo b Cu c V d X e Y f Z g O h wherein P, Mo, Cu, V and O are phosphorus, molybdenum, copper, vanadium and oxygen, respectively, X is at least one element selected from the group consisting of arsenic, antimony, bismuth, germanium, zirconium, tellurium and silver, Y is at least one element selected from the group consisting of iron, zinc, chromium, magnesium, tantalum, manganese, barium, boron, gallium, cerium and lanthanum, Z is at least one element selected from the group consisting of potassium, rubidium, cesium and thallium, a, b, c, d, e, f, g and h are an atomic ratio of each element, and when b is 12, a is 0.5 to 3, c is 0.01 to 2, d is 0.01 to 3, e is 0.01 to 3, f is 0 to 3, g is 0.01 to 2 and h is the number of oxygen atoms necessary to satisfy the valence of each component, an improvement comprising adding 0.05 to 1.0 mole of nitric acid based on 12 moles of a molybdenum atom to a slurry containing materials for the catalyst components. According to the present invention, a catalyst for gas-phase catalytic oxidation excellent in the conversion of methacrolein and selectivity for methacrylic acid is obtained.

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