Process for preparing halogen magnesium alanate and use thereof

Details Process for preparing halogen magnesium alanate and use thereof Process for preparing halogen magnesium alanate and use thereof

C - Chemistry, Metallurgy

01

B

23/133, 23/294,

C01B 6/24 (2006.01) C01B 9/00 (2006.01) C07B 31/00 (2006.01) C07C 1/26 (2006.01) C07C 29/14 (2006.01) C07C 29/143 (2006.01) C07C 29/147 (2006.01)

Patent

CA 1306597

PROCESS FOR PREPARING HALOGEN MAGNESIUM ALANATE AND USE THEREOF Abstract of the Disclosure The invention relates to a process for pre- paring halogen magnesium alanates XMgAlH4 (X = Cl, Br, I) from aluminum halide and magnesium hydride, which process is characterized in that an aluminum halide AlX3 (X = Cl, Br, I) is reacted with a magnesium hydride in a solvent, said magnesium hydride having been prepared from magne- sium and hydrogen in a solvent in the presence of homo- geneous catalysts consisting of a halide of a metal of the Subgroups IV to VIII of the Periodic System and of an organomagnesium compound or a magnesium hydride, respect- ively, and in the presence of a polycylic aromatic or of a tertiary amine and optionally in the presence of a magnesium halide MgX2 (X = C1, Br, I) and to the use of the halogen magnesium alanates thus formed.

520128

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