Process for preparing n-alkylethylene diamine

C - Chemistry – Metallurgy – 07 – C

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260/607.9

C07C 209/08 (2006.01)

Patent

CA 1128070

27,864 PROCESS FOR PREPARING N-ALKYLETHYLENEDIAMINES ABSTRACT OF THE DISCLOSURE This disclosure describes a novel process for pre- paring N-alkylethylenediamines wherein the alkyl is from C3 to about C6 which are useful as intermediates for purifying penicillins. N-alkylethylenediamines are also useful for preparing penicillins and cephalosporins. More particularly, the invention relates to a pro- cess for the efficient reaction of an alkyl halide wherein the alkyl is from C3 to about C6 and ethylenediamine and the recovery of anhydrous, ethylenediamine-free N-alkylethylene- diamines therefrom.

332700

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