Process for preparing n-methylated methyl dihydrolysergate...

C - Chemistry – Metallurgy – 07 – D

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260/206.1

C07D 457/04 (2006.01)

Patent

CA 1246552

BREVET D'INVENTION PROCEDE DE PREPARATION DES DERIVES N-METHYLES DU DIHYDROLYSERGATE DE METHYLE OU DU METHOXYLUMILYSERGATE DE METHYLE RHONE-POULENC SANTE ABREGE Procédé de préparation des produits de formule générale (I) par action d'un agent de méthylation et d'un sel quaternaire en présence d'un alcoolate métallique solide ou d'un hydrure alcalin et d'un ester de formule générale (IV) ou d'un orthoester de formule générale (V) sur un produit de formule générale (II). Dans les formules générales (I) et (IV) R1 représente un atome d'hydrogène ou un radical méthoxy. Image (I) (II) R2-COO CH3 (IV) R3-C(OCH3)3 (V)

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