Process for preparing n-phenyl-n-methoxyacetyl-dl-alanine...

C - Chemistry – Metallurgy – 07 – C

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260/476.3

C07C 231/14 (2006.01) C07C 235/16 (2006.01)

Patent

CA 2032146

PROCESS FOR PREPARING N-PHENYL-N-METHOXYACETYL- -DL-ALANINE-METHYLESTER DERIVATIVES Abstract The invention relates to a new process for the preparation of N-phenyl-N-methoxy- -acetyl-DL-alanine methylester of the general formula (I) wherein R stands for hydrogen atom or C1-C4 alkyl group The process discloses the acylation of a substituted aniline of the general formula (II) with a mixture of methoxyacetic acid and phos- phorous trichloride in a solvent then alkylation of the obtained N-methoxyacetyl-aniline deri- vative of the general formula (Ill) with an alkyl halogenide in the presence of an alkali metal, alkali metal alcoholate, alkali metal amide or complex metalhydride..

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