C - Chemistry – Metallurgy – 07 – C
Patent
C - Chemistry, Metallurgy
07
C
260/476.3
C07C 231/14 (2006.01) C07C 235/16 (2006.01)
Patent
CA 2032146
PROCESS FOR PREPARING N-PHENYL-N-METHOXYACETYL- -DL-ALANINE-METHYLESTER DERIVATIVES Abstract The invention relates to a new process for the preparation of N-phenyl-N-methoxy- -acetyl-DL-alanine methylester of the general formula (I) wherein R stands for hydrogen atom or C1-C4 alkyl group The process discloses the acylation of a substituted aniline of the general formula (II) with a mixture of methoxyacetic acid and phos- phorous trichloride in a solvent then alkylation of the obtained N-methoxyacetyl-aniline deri- vative of the general formula (Ill) with an alkyl halogenide in the presence of an alkali metal, alkali metal alcoholate, alkali metal amide or complex metalhydride..
Agocs Pal
Kolonics Zoltan
Legradi Laszlo
Molnar Sandor
Nagy Lajos
Nitrokemia Ipartelepek
Sim & Mcburney
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