C - Chemistry – Metallurgy – 07 – C
Patent
C - Chemistry, Metallurgy
07
C
202/100, 260/648
C07C 43/04 (2006.01) C07C 41/06 (2006.01)
Patent
CA 1081261
ABSTRACT OF THE DISCLOSURE An improved process for the preparation of pure methyl tert.-butyl ether. Isobutene or isobutene-containing hydrocarbon mixtures are reacted with methanol in a molar ratio of 1:1 to 1:2 in the liquid phase at temper- atures of between 30° and 100°C. on sulfonated, strongly acidic, macroporous organic ion exchange resins. After separation of the unreacted hydrocarbons, the reaction mixture is distilled under pressure; the methanol-containing distillate formed during the distillation is recycled into the zone of the reaction between methanol and isobutene; and pure methyl tert.-butyl ether is withdrawn from the sump of the distillation column.
281866
Droste Wilhelm
Muller Wolfgang
Obenaus Fritz
Streubel Wolf
Zolffel Michael
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