Process for preparing substituted tetralones

Details Process for preparing substituted tetralones Process for preparing substituted tetralones

C - Chemistry, Metallurgy

07

C

260/576.6

C07C 49/755 (2006.01) C07C 45/28 (2006.01)

Patent

CA 1243688

ABSTRACT PROCESS FOR PREPARING SUBSTITUTED TETRALONES 6-Alkoxytetralones are prepared by gradually adding a persulfate to a heated mixture of a 6-alkoxy- tetralin, a salt of a divalent metal, and a tertiary amine and maintaining the 6-alkoxytetralin in intimate admixture with the persulfate until it has been oxidized to the corresponding 6-alkoxytetralone. The reaction is preferably conducted in solution or dispersion. Preferred reaction ingredients are 6-methoxytetralin, cupric sul- fate, an alkylpyridine, and sodium persulfate.

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