Process for preparing terephthalic acid

Details Process for preparing terephthalic acid Process for preparing terephthalic acid

C - Chemistry, Metallurgy

07

C

260/510.8

C07C 63/26 (2006.01) B01J 27/08 (2006.01) C07C 51/265 (2006.01)

Patent

CA 1114835

TITLE OF THE INVENTION: PROCESS FOR PREPARING TEREPHTHALIC ACID ABSTRACT OF DISCLOSURE A process for the continuous preparation of pure terephthalic acid by oxidation of p-xylene with molecular oxygen in acetic acid solvent comprising conducting the oxidation at a tem- perature of 205 to 230°C in the presence of an oxidation catalyst comprising (a) a cobalt compound in an amount of at least 120 ppm and less than 200 ppm as cobalt based on the weight of solvent, (b) a manganese compound sufficient to provide a manganese to cobalt weight ratio of 0.5 to 1.5 and (c) a bromine compound selected from hydrogen bromide, cobalt bromide and manganese bromide in an amount of 200 to 1,000 ppm as bromine based on the weight of solvent, while the water content of the liquid phase of the reaction system is kept at 4 to 14 percent by weight. - 1 -

313864

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