Process for producing dialkyl phosphorochloridothionates

Details Process for producing dialkyl phosphorochloridothionates Process for producing dialkyl phosphorochloridothionates

C - Chemistry, Metallurgy

07

F

260/460.1

C07F 9/206 (2006.01) C07F 9/20 (2006.01)

Patent

CA 1168254

PROCESS FOR PRODUCING DIALKYL PHOSPHOROCHLORIDOTHIONATES ABSTRACT OF THE INVENTION The process of producing a lower alkyl ester of phosphorochloridothioic acid by the chlorination of alkyl esters of dithiophosphoric acid in which the chlorine added after the addition of from .63 to .86 moles of chlorine per mole of phosphorodithioic acid is diluted with an inert gas. The disclosed process improves product yields, and purity, and advantageously provides for simple HC1 recovery. C-6131

386054

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