Process for producing glutamine derivative

Details Process for producing glutamine derivative Process for producing glutamine derivative

C - Chemistry, Metallurgy

07

C

C07C 237/22 (2006.01) C07C 231/02 (2006.01) C07C 231/10 (2006.01)

Patent

CA 2146708

N-chloroacetylglutamine is produced by reacting chloroacetyl chloride with an alkaline aqueous solution of glutamine in the presence of a water-immiscible organic solvent, separating an aqueous layer by liquid-liquid separation, and crystallizing N-chloroacetyl-glutamine from the aqueous layer under acidic conditions. N-Chloroacetyl- glutamine useful as an intermediate for producing glycyl-L- glutamine which has higher stability than L-glutamine and is used as a component of an infusion solution can be obtained with high efficiency at low cost.

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