Process for producing n-glycyltyrosine and its crystal...

Details Process for producing n-glycyltyrosine and its crystal... Process for producing n-glycyltyrosine and its crystal...

C - Chemistry, Metallurgy

07

K

C07K 5/062 (2006.01) C07C 231/12 (2006.01) C07C 233/47 (2006.01) C07K 1/02 (2006.01) C07K 5/06 (2006.01)

Patent

CA 2268586

Provided is a process for efficiently producing N-glycyltyrosine of high purity represented by the following formula: Image a salt thereof, or a solvate thereof, which comprises adding dropwise to an aqueous suspension of tyrosine or a salt thereof 2 equivalents or more of a haloacetyl halide and an aqueous solution of an inorganic base simultaneously in the presence or absence of an organic solvent, and subjecting the resulting N-haloacetyltyrosine to a reaction with an ammonium ion. Also provided are N-glycyl-L-tyrosine dihydrate having the crystal structures showing specific diffraction patterns in X-ray powder diffraction and processes for producing the same which are characterized by comprising crystallizing the dihydrate from an ethanol-water mixed solvent or water.

Affiliated with

Also associated with

Rating

Process for producing n-glycyltyrosine and its crystal... does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Process for producing n-glycyltyrosine and its crystal..., we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Process for producing n-glycyltyrosine and its crystal... will most certainly appreciate the feedback.

Rate now

Comments { 0 }

Profile ID: LFCA-PAI-O-1950494