Process for production of dialkali metal phosphates by ion...

C - Chemistry – Metallurgy – 01 – B

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C01B 25/30 (2006.01) B01J 39/00 (2006.01) B01J 47/00 (2006.01)

Patent

CA 1275559

ABSTRACT OF THE DISCLOSURE A process for the production of dialkali metal phosphates by ion exchange is disclosed. The process is carried out by first ammoniatinq a water- soluble phosphate source such as phosphoric acid or monocalcium phosphate. The resulting ammoniated phosphate solution is then contacted with a weak cation exchange resin in the alkali metal form to produce the dialkali metal phosphate as well as an ammonium-loaded weak cation exchange resin. The cation exchange resin is regenerated by contacting it with an alkali metal salt solution which effects an exchange of alkali metal for ammonium to produce a regenerated weak cation exchange resin in the alkali metal form as well as a water-soluble ammonium salt corresponding to the initial alkali metal salt. The process may be carried out in conventional fixed or pulsed bed ion exchange systems although it is most advantageously carried out in an Advanced Separation Device which is a multi- chambered device which enables the process to be carried out both continuously and with a greater degree of efficiency than is possible using conventional ion exchange systems.

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