Process for reclaiming a contaminated electrolyte from an...

C - Chemistry – Metallurgy – 25 – B

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C25B 15/08 (2006.01) B01D 21/01 (2006.01) C25B 1/24 (2006.01)

Patent

CA 2658543

A process for reclaiming a contaminated electrolyte in an electrolytic cell used in the production of gaseous fluorine. The contaminated electrolyte is a mixture of potassium bifluoride and hydrofluoric acid having metal ions therein. The process has the following steps: a) removing the contaminated electrolyte from the cell to a treatment tank; b) adding a lithium compound to the contaminated electrolyte in the treatment tank to induce settlement of at least part of the metal ions; c) allowing the metal ions to settle to the bottom of the treatment tank; d) removing the settled metal ions from the bottom of the treatment tank to form a reclaimed electrolyte; and e) returning the reclaimed electrolyte to the cell.

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