Process for reducing the free aldehyde content in n-alkylol...

C - Chemistry – Metallurgy – 07 – C

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C07C 233/20 (2006.01) A61L 15/24 (2006.01) C07C 231/12 (2006.01) C07C 235/76 (2006.01) C07C 271/16 (2006.01) C07D 209/48 (2006.01) C07D 317/30 (2006.01) C07D 319/06 (2006.01) C08F 6/00 (2006.01) C08F 218/08 (2006.01) C08K 5/20 (2006.01) D04H 1/64 (2006.01) D06M 11/80 (2006.01) D06M 15/263 (2006.01) D06M 15/285 (2006.01) D06M 15/29 (2006.01) D06M 15/333 (2006.01) D06M 15/693 (2006.01) D21H 17/36 (2006.01) D21H 17/39 (2006.01)

Patent

CA 2116318

In a process for the preparation of N-alkylol amide monomers wherein a polymerizable amide is reacted with an aldehyde, the improvement which comprises adjusting the pH of the resulting N-alkylol amide monomer to pH 10-11 and adding thereto an alkali or alkali earth metal borohydride at a temperature of -10 to 25°C so as to convert the residual free aldehyde in the equilibrium mixture to the corresponding alcohol.

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