Process for seed crystal preparation for phosphoric acid...

C - Chemistry – Metallurgy – 01 – B

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C01B 25/234 (2006.01) C01B 25/20 (2006.01) C01B 25/24 (2006.01)

Patent

CA 1265315

Abstract Process For Seed Crystal Preparation For Phosphoric Acid Crystallization The present invention relates to the processing of phosphoric acid by crystallization starting with phosphoric acid and adding relatively large amounts of fine, relatively pure seed crystals to acid which has been cooled to supersaturated conditions. Crystal- lization thereafter proceeds under conditions which substantially favor growth on the seeds which are added and disfavor secondary nucleation. The present invention particularly describes a seed crystal gen- erator for use in the foregoing process in which rela- tively high purity phosphoric acid, containing 60% to 66% P2O5 is cooled to a temperature of at least 5 to 10°C below zero and thereafter nucleated under agita- tion in a crystallizing vessel of short residence time.

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