Process for separating 1-tetradecene from triethylaluminum

Details Process for separating 1-tetradecene from triethylaluminum Process for separating 1-tetradecene from triethylaluminum

C - Chemistry, Metallurgy

07

F

202/101, 260/432

C07F 5/06 (2006.01) B01D 3/10 (2006.01) C07C 2/88 (2006.01) C07C 7/04 (2006.01) C07C 11/02 (2006.01)

Patent

CA 2015067

Tetradecene-1 can be rectified from a mixture containing 1-tetradecene and triethyl aluminum ("TEA") which has about the same normal boiling point as 1-tetradecene by conducting the distillation in a rectification column under sufficient vacuum (e.g., 5-30 torr) such that the temperature in the rectification section of the column is in the range of 200-250°F. The TEA which normally boils at about the same temperature as 1-tetradecene will exist as a dimer permitting part of the tetradecene to distill overhead and most of the TEA to exit the bottom of the column.

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