Process for sulfonation and apparatus therefor

C - Chemistry – Metallurgy – 07 – B

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23/387, 260/465,

C07B 45/02 (2006.01) B01J 10/02 (2006.01)

Patent

CA 1072977

ABSTRACT OF THE DISCLOSURE Sulfonation of a sulfonatable organic compound is effected by means of a two-stage reaction with an SO3- containing gas, in which the first-stage reaction is carried out by flowing, in parallel flow relation, said organic compound and said SO3-containing gas upwardly into the lower ends of a plurality of vertically positioned cylinders of double-cylinders, and the second-stage reaction is carried out by the steps of collecting the reaction product of the first-stage reaction, adding fresh SO3-containing gas to the reaction product thus collected and flowing in parallel flow arrangement the reaction mixture downwardly into the upper end of a vertically positioned cylinder or double-cylinder.

256974

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