Process for synthesis of azines, its application to...

C - Chemistry – Metallurgy – 07 – C

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23/215, 260/591

C07C 241/02 (2006.01) C01B 21/16 (2006.01) C07C 243/10 (2006.01) C07C 249/00 (2006.01) C07C 251/88 (2006.01)

Patent

CA 2017358

L'invention concerne dans un procédé continu de synthèse d'azines à partir d'eau oxygénée, d'ammoniac et d'un réactif portant un groupe CO, (i) une solution de travail circulant en boucle entre le réacteur d'azines et un dispositif de traitement et (ii) l'introduction d'un produit choisi de préférence parmi l'acide acétique, l'acétate d'ammonium et l'acétonitrile. Les azines sont hydrolysées pour obtenir de l'hydrate d'hydrazine. Ce procédé est beaucoup plus simple que dans l'art antérieur et permet d'assurer une production continue et constante d'azines sans avoir à contrôler en détail la solution de travail.

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