Process for synthesizing pharmaceutically active disulfide...

Details Process for synthesizing pharmaceutically active disulfide... Process for synthesizing pharmaceutically active disulfide...

C - Chemistry, Metallurgy

07

C

C07C 309/66 (2006.01) C07C 319/24 (2006.01) C07C 327/22 (2006.01) C07F 9/32 (2006.01) C07F 9/38 (2006.01) C07C 323/66 (2006.01)

Patent

CA 2483775

A process for synthesizing pharmaceutically active disulfides, particularly Dimesna and certain derivatives thereof. The process includes reacting an alkylene salt with a sulfurating reagent, then alkalizing the intermediate and flowing oxygen through the mixture to produce the final compound in high yield.

L'invention concerne un procédé de synthèse de disulfure actifs pharmaceutiquement, en particulier de Dimesna et de certains dérivés. Le procédé consiste à faire réagir un sel d'alkylène avec un réactif de sulfuration, ensuite à alkaliser l'intermédiaire et à faire s'écouler de l'oxygène dans le mélange pour produire le composé final à haut rendement.

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