Process for the adiabatic preparation of mononitrotoluenes

Details Process for the adiabatic preparation of mononitrotoluenes Process for the adiabatic preparation of mononitrotoluenes

C - Chemistry, Metallurgy

07

C

C07C 205/06 (2006.01) C07C 201/08 (2006.01)

Patent

CA 2142257

Mononitrotoluenes can be prepared by intensively mixing together toluene, nitric acid, sulphuric acid and water, simultaneously or successively in their total amount, and, in the case of continuous preparation, redispersing the mixture at least twice, for which purpose a mixing energy of 1 to 40 watts per litre of the total reaction mixture, preferably 3 to 30 W/l, is employed per volume of the reactor, and, for the continuous procedure, the back-mixing is substantially repressed. Adiabatic reaction conditions are maintained.

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