Process for the distillative separation of tertiary alkyl...

Details Process for the distillative separation of tertiary alkyl... Process for the distillative separation of tertiary alkyl...

C - Chemistry, Metallurgy

07

C

202/95

C07C 407/00 (2006.01)

Patent

CA 1158195

Abstract of the Disclosure A process for the distillative separation of tertiary alkyl hydroperoxides of the formula R-00H wherein R is a tertiary alkyl group with 4 to 6 carbon atom from the corresponding di-tertiary alkyl peroxides resulting during their preparation, which process comprises neutralizing the reaction mixture resulting during the preparation of the tertiary alkyl hydroperoxide, subjecting same to vacuum dis- tillation in the presence of water at a temperature of less than about 45°C and recovering the purified tertiary alkyl hydroperoxide as a bottoms product.

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