Process for the manufacture of lh-rh and lh-rh analogs using...

Details Process for the manufacture of lh-rh and lh-rh analogs using... Process for the manufacture of lh-rh and lh-rh analogs using...

C - Chemistry, Metallurgy

07

K

530/7.2

C07K 7/23 (2006.01) C07K 5/078 (2006.01)

Patent

CA 1144160

HOE 79/F 027 PROCESS FOR THE MANUFACTURE OF LH-RH AND LH-RH ANALOGS USING ?lu-His(DnP)-OH Abstract of the Disclosure: Process for the manufacture of LH-RH and LH-RH ana- logs, which cornprises reacting ?lu-His(DnP)-OH with the corresponding peptide having a free amino group and protected carboxy groups in a solvent as used in peptide chemistry and with the addition of 3-hydroxy-4-oxo-3,4-di- hydro-1,2,3-benzotriazine (HOObt) and a a,arbodiimide and then splitting off the Dnp-(2,4-dinitrophenyl) group. The invention also provides a new dipeptide, i.e. ?lu-His(Dnp)- OH.

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